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Effect of Shear on the Crystallization of the Poly(ether ether ketone)
Zhao, GY; Men, YF; Wu ZH(吴忠华); Wu, ZH; Ji, XL; Jiang, W
2010
发表期刊JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS
卷号48期号:2页码:#REF!
通讯作者Ji, XL (reprint author), Chinese Acad Sci, Changchun Inst Appl Chem, State Key Lab Polymer Phys & Chem, Changchun 130022, Peoples R China.
文章类型Article
摘要The effect of shear on the crystallization behavior of the poly(ether ether ketone) (PEEK) has been investigated by means of ex situ wide-angle X-ray diffraction (WAXD), small-angle X-ray scattering, and differential scanning calorimetry (DSC). The changes of the intensity of WAXD patterns along shear direction of the PEEK induced by short-term shear were observed when the samples crystallized at 330 degrees C. The results showed that the dimensions of the crystallites perpendicular to the (110) and (111) planes reduced with the increase of shear rate, whereas the dimensions of the crystallites perpendicular to (200) plane increased with the increase of shear rate. Moreover, increasing shear rate can lead to the increase of the crystallinity as well as the average thickness of the crystalline layers. Correspondingly, a new melting peak at higher temperature was found during the subsequent DSC scanning when the shear rate was increased to 30 s(-1). (C) 2009 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 48: 220-225, 2010
关键词crystallization poly(ether ether ketone) (PEEK) SAXS shear WAXD
学科领域Polymer Science
DOI10.1002/polb.21851
收录类别SCI
WOS类目Polymer Science
WOS记录号WOS:000273581500015
引用统计
被引频次:7[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.ihep.ac.cn/handle/311005/227015
专题多学科研究中心
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GB/T 7714
Zhao, GY,Men, YF,Wu ZH,et al. Effect of Shear on the Crystallization of the Poly(ether ether ketone)[J]. JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS,2010,48(2):#REF!.
APA Zhao, GY,Men, YF,吴忠华,Wu, ZH,Ji, XL,&Jiang, W.(2010).Effect of Shear on the Crystallization of the Poly(ether ether ketone).JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS,48(2),#REF!.
MLA Zhao, GY,et al."Effect of Shear on the Crystallization of the Poly(ether ether ketone)".JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS 48.2(2010):#REF!.
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