Tribological study of a highly hydrolytically stable phenylboronic acid ester containing benzothiazolyl in mineral oil
Li, ZP; Li, XF; Zhang, YW; Ren, TH; Zhao, YD; Zeng, XQ; van der Heide, E;赵屹东
刊名APPLIED SURFACE SCIENCE
2014
卷号308页码:91-99
关键词Phenylboronic acid ester Heterocyclic compound Hydrolytic stability Anti wear Surface analysis
学科分类Chemistry; Materials Science; Physics
DOI10.1016/j.apsusc.2014.04.116
英文摘要A novel long chain alkyl phenylboronic acid ester containing heterocyclic compound, bis (1(benzothiazol-2-ylthio) propan-2-yl)-4-dodecylphenylboronic acid ester (DBBMT), was synthesized and characterized. The hydrolytic stability of the DBBMT was evaluated and the results show that DBBMT is of outstanding hydrolytic stability compared with normal borate esters, which indicates that the designed molecular structure, by introducing benzene ring to conjugate with the electron-deficient boron and the benzothiazole as a hinder group, is effective on obtaining a hydrolytically stable long chain alkyl phenylboronic acid ester. The tribological properties of DBBMT and ZDDP in mineral base oil were evaluated using a four-ball tribometer, which suggests that the DBBMT possesses comprehensive tribological properties and could be a potential candidate for the replacement of ZDDP. Furthermore, in order to understand the tribological behaviors, the worn surface was analyzed by X-ray photoelectron spectroscopy (XPS) and X-ray absorption near edge structure (XANES) spectroscopy. The results indicate that the elements S, B, O and Fe perform complicated tribochemical reactions to form the compact tribological film composed of B2O3, FeS, Fe3O4 and FeSO4. (C) 2014 Elsevier B.V. All rights reserved.
收录类别SCI
WOS记录号WOS:000336599900013
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被引频次:15[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.ihep.ac.cn/handle/311005/224830
专题中国科学院高能物理研究所_多学科研究中心_期刊论文
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Li, ZP,Li, XF,Zhang, YW,et al. Tribological study of a highly hydrolytically stable phenylboronic acid ester containing benzothiazolyl in mineral oil[J]. APPLIED SURFACE SCIENCE,2014,308:91-99.
APA Li, ZP.,Li, XF.,Zhang, YW.,Ren, TH.,Zhao, YD.,...&van der Heide, E;赵屹东.(2014).Tribological study of a highly hydrolytically stable phenylboronic acid ester containing benzothiazolyl in mineral oil.APPLIED SURFACE SCIENCE,308,91-99.
MLA Li, ZP,et al."Tribological study of a highly hydrolytically stable phenylboronic acid ester containing benzothiazolyl in mineral oil".APPLIED SURFACE SCIENCE 308(2014):91-99.
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