Determination of Nine Hazardous Elements in Textiles by Inductively Coupled Plasma Optical Emission Spectrometer after Microwave-Assisted Dilute Nitric Acid Extraction
Chen F(陈飞); 徐殿斗;Chen, F; Xu, DD; Tang, XP; Cao, J; Liu, YT; Deng, J
刊名SPECTROSCOPY AND SPECTRAL ANALYSIS
2012
卷号32期号:1页码:239-243
关键词ICP-OES Heavy metals Textiles, Microwave-assisted extraction
学科分类Spectroscopy
DOI10.3964/j.issn.1000-0593(2012)01-0239-05
英文摘要Textiles are easily contaminated by heavy metals in the course of processing. In order to monitor the quality of textiles, a new method was developed for simultaneous determination of arsenic, antimony, lead, cadmium, chromium, cobalt, copper, nickel and mercury in textiles by inductively coupled plasma optical emission spectrometry (ICP-OES) after microwave-assisted dilute nitric acid extraction. After optimizing extraction conditions, we ultimately selected 5% nitric acid as extractant and 5 mm as extraction time with the extraction temperature of 120 degrees C and instrument power of 400W in the microwave-assisted extraction procedure. Nine hazardous elements were detected sequentially by ICP-OES. The results showed that the detection limits were 0.3 similar to 15 mu g . L(-1) and the recoveries 73.6%similar to 105% with the RSDs (n=3) of 0.1%similar to 3%. The proposed method was successfully used to determine nine elements in cotton, wool, terylene and acrylic.
收录类别SCI
WOS记录号WOS:000298900300054
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被引频次:3[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.ihep.ac.cn/handle/311005/223903
专题中国科学院高能物理研究所_核技术应用研究中心_期刊论文
中国科学院高能物理研究所_多学科研究中心
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Chen F,徐殿斗;Chen, F,Xu, DD,et al. Determination of Nine Hazardous Elements in Textiles by Inductively Coupled Plasma Optical Emission Spectrometer after Microwave-Assisted Dilute Nitric Acid Extraction[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS,2012,32(1):239-243.
APA 陈飞.,徐殿斗;Chen, F.,Xu, DD.,Tang, XP.,Cao, J.,...&Deng, J.(2012).Determination of Nine Hazardous Elements in Textiles by Inductively Coupled Plasma Optical Emission Spectrometer after Microwave-Assisted Dilute Nitric Acid Extraction.SPECTROSCOPY AND SPECTRAL ANALYSIS,32(1),239-243.
MLA 陈飞,et al."Determination of Nine Hazardous Elements in Textiles by Inductively Coupled Plasma Optical Emission Spectrometer after Microwave-Assisted Dilute Nitric Acid Extraction".SPECTROSCOPY AND SPECTRAL ANALYSIS 32.1(2012):239-243.
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